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Laboratory Testing

Laboratory Testing & Assay

Independent, ISO 17025 accredited laboratory analysis for gold and rough diamonds. Fire assay, XRF, ICP-MS spectrometry — the definitive methods for commercial settlement.

ISO 17025 Accredited
LBMA Approved Methods
Legally Binding Reports
Chain of Custody

Independent Commercial Settlement

We coordinate comprehensive analytical services through internationally accredited laboratories. Our partner facilities provide testing for all precious metals and minerals — from exploration samples through to commercial settlement.

Laboratory expertise includes classical assay methods such as gravimetric (wet chemistry) and fire assay, as well as instrumental techniques including Inductively Coupled Plasma (ICP-OES/ICP-MS) and X-Ray Fluorescence (XRF).

Every test result is legally binding and admissible for commercial settlement, insurance claims, and customs valuation.

Purity Analysis for Commercial Settlement

Definitive determination of gold content for buy/sell transactions with legally binding results.

Umpire & Arbitration Analysis

Independent third-party testing to resolve disputes when buyer and seller results differ.

Full Chain of Custody

Complete sample tracking from collection through testing to certificate issuance.

Testing Standards

ISO 17025 Accredited

International laboratory quality standard

LBMA Approved Methods

London Bullion Market standards

Externally Audited

Independent quality assurance

Legally Binding Reports

Admissible for settlement & customs

Testing Methods

Different testing methods serve different purposes. Here's what each involves and when it's used.

XRF Analysis

X-Ray Fluorescence provides rapid, non-destructive elemental analysis. Ideal for screening.

Capabilities
  • Multi-element detection (Au, Ag, Pt, Pd)
  • Surface composition analysis
  • Rapid results (minutes)
  • Non-destructive testing
  • Portable field testing available
Accuracy±0.1-0.5%
TurnaroundSame day
Sample TypeNon-destructive

ICP-MS / ICP-OES

Inductively Coupled Plasma Spectrometry for trace element detection at PPM/PPB levels.

Capabilities
  • Trace impurity detection
  • Full elemental composition
  • PPM/PPB sensitivity
  • Multi-element simultaneous analysis
  • Platinum group metals (PGM)
DetectionPPB level
Turnaround2-3 days
Sample TypeDestructive

Gravimetric Analysis

Classical wet chemistry method using precipitation and weighing for comprehensive analysis.

Applications
  • Silver determination
  • Base metal quantification
  • Verification of other methods
  • Referee analysis
Accuracy±0.02%
Turnaround3-5 days
Sample TypeDestructive

Density / Specific Gravity

Archimedes principle testing to detect tungsten cores or other counterfeiting methods.

Detects
  • Tungsten-filled bars
  • Plated base metal
  • Hollow cores
  • Mixed alloy composition
Gold Density19.32 g/cm³
TurnaroundSame day
Sample TypeNon-destructive

Umpire / Arbitration

Independent third-party analysis when buyer and seller assay results disagree.

Process
  • Independent sample collection
  • Blind testing protocol
  • Referee methodology
  • Legally binding results
StandardLBMA Rules
Turnaround5-7 days
BindingYes

Fire Assay: The Gold Standard

Fire assay has been the definitive method for gold determination for over 500 years. It remains the "referee" method used by refineries, central banks, and trading houses worldwide.

The method completely separates gold from all other elements through a series of high-temperature fusions and chemical separations, then weighs the pure gold remaining.

1

Sample Preparation & Fusion

The sample is mixed with flux containing lead oxide, borax, and silica, then heated to 1,000°C+.

2

Cupellation

The lead button is heated in a porous cupel. Lead oxide is absorbed, leaving a "prill" of gold and silver.

3

Inquartation & Parting

Silver is added to achieve a 3:1 ratio. The alloy is dissolved in nitric acid, leaving gold intact.

4

Gravimetric Finish

The remaining pure gold is washed, annealed, and weighed on a precision microbalance.

Fire Assay Accuracy

The most precise method for gold determination

Purity Accuracy 99.99%
±0.01%
Precision Tolerance
3-5
Days Turnaround
500+
Years of Use
100%
Settlement Acceptance

Fire assay is required by LBMA Good Delivery rules and accepted by all major refineries worldwide.

ASSAY CERTIFICATE

ISO 17025 Accredited Laboratory

LAB-2024-XXXXX
DD/MM/YYYY
Gold Dore Bars
1,000.00 g
96.45%
964.50 g
Fire Assay with Gravimetric Finish (LBMA Approved)
Ag: 2.8%, Cu: 0.5%, Fe: 0.15%, Other: 0.1%

What Your Certificate Includes

Every assay certificate from our partner laboratories contains the information required for commercial settlement, customs clearance, and insurance purposes.

  • Unique Certificate Number — Traceable reference for all parties
  • Gross Weight — Total weight of sample as received
  • Purity / Fineness — Gold content as percentage
  • Fine Weight — Calculated pure gold content
  • Testing Methodology — Fire assay, XRF, ICP, etc.
  • Impurity Analysis — Silver, copper, and other elements
  • Laboratory Accreditation — ISO 17025 certification
  • Chain of Custody Record — Sample tracking documentation

Rough Diamond Analysis

Professional evaluation of rough diamonds through accredited gemological laboratories.

Cut Potential

Assessment of optimal cutting strategy and expected yield from rough stones.

Color Grading

D-Z color scale evaluation and detection of fancy colors or treatments.

Clarity Analysis

Internal characteristics mapping, inclusion identification, and clarity potential.

Carat Weight

Precision weighing and documentation for customs and valuation purposes.

Testing Timeline

From sample collection to certificate delivery — here's the typical process.

Sample Collection

Secure collection with chain of custody

Day 1

Lab Transport

Insured transport to accredited facility

Day 1-2

Testing

Fire assay, XRF, ICP-MS analyses

Day 3-5

QA Review

Quality assurance and certificate prep

Day 5-6

Certificate Issued

Official assay certificate delivered

Day 6-7

Our Role

To be clear about what we do and don't do regarding laboratory testing.

What We Do

  • Coordinate testing through ISO 17025 accredited laboratories
  • Arrange secure sample collection and transport
  • Recommend appropriate testing methods for your transaction
  • Ensure proper chain of custody documentation
  • Facilitate communication between parties and laboratories
  • Provide certificates to all relevant parties

What We Don't Do

  • Operate our own laboratory facilities
  • Perform testing ourselves
  • Issue assay certificates in our name
  • Guarantee specific purity results
  • Interfere with independent laboratory processes

Common Questions

Why is fire assay the preferred method?

Fire assay completely separates gold from all other elements and weighs the pure gold remaining. This gravimetric finish provides the highest accuracy.

Is XRF testing accurate enough?

XRF is excellent for screening but only analyzes the surface. For commercial settlement, fire assay is required because it tests the entire sample.

What happens if results are disputed?

We can arrange umpire (arbitration) analysis through an independent third laboratory. Results are legally binding under LBMA rules.

How much sample is needed?

Fire assay typically requires 30-50 grams. XRF can work with any size. For large lots, multiple samples are taken and averaged.

Are the laboratories independent?

Yes. We work with externally audited, ISO 17025 accredited laboratories that operate independently. We have no interest in results.

Can I choose the laboratory?

Yes. You can select from our network of partner laboratories, or specify a particular facility if you have a preference.

Ready to Verify Your Precious Metals?

We'll coordinate professional testing through accredited laboratories and ensure you get legally binding results.

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